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I
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I .
O. H. M. B.
Ar DfnUp ifinittmr.
LABORATORY
INLAND REVENUE DEPARTMENT
OTTAWA, CANADA
BULLETIN ISTo. 167
SPIRITUS AETHERIS NITROSI
9170—1
LABORATORY
Ot TBI
INLAND REVENUE DEPARTMENT
OTTAWA. CANADA
BULLETIN No. 1(J7
SPIKITUS AETHERIS NITROSI
Ottawa, December 9, 1908.
W. J. Gerald, Esq.,
Deputy Minuter of Inland Revenue.
Sir,— I have the honour to report upon 77 samples of Spiritui A$th«ru Xilrtmi or
Spirit of Nitrous Ether, collected throughout Canada in OctoVyr iaat.
Thin important drug consiHts essentially of a solution of ethyl nitrite in alcohol.
The directions given for its preparation in the British Pharmacopoeia are such aa to
produce a solution answering the following official tests. Treated for deoompontion
of the nitrite, at normal temperature and pressure, it should yield, ' when freshly
prepared, at least 6J, but not more than 7, volumes of nitric oxide gas, corresponding to
at least 2i parte by weight of ethyl nitrite in 100 parts by weight of the spirit : and
even after it has been kept for some time, and the vessel containing it has occasional*
been opened, it should yield not much less than 6 times its volume of the gai, correspond-
ing to nearly 2 per cent by weight of ethyl nitrite or a minimum of IJ per cent'
The United States Fbarmacopceia reijuires 4 per cent of ethyl nitrite in the freshly
prepared article, corresponding to 1 1 times its volume of nitric oxide. The percentage
content in ethyl nitrite, as given in the table of analyses, is calculated upon the basis
of 4 per cent othyl nitrite, equivalent to 11 volumes of nitric oxide.
It may be incidentally noted that Dr. Leech (The LuTuset, London, Feb, 1889) has
shown that this preparation owes ite characteristic physiological properties to ite content
of ethyl nitrite. But, apart from this consideration, so long as the article remuns
pbarmacopoeal, it is the duty of this Department, as administering the Adulteration
Act, to see that the requirements of the Pharmacopceias are met The following per-
centages of ethyl nitrite are distinctly required by the pharmacopoeias in question.
BRITISH PHARMACOP(EIA.
For freshly prepared Spirite of Nitrous Ether.
Per cent
Maximum 2 ■ 56
Minimum • 2-27
For spirits ' kept some time, Ac'
Minimum 1 ' 76
u-
s
UNITU) BTATM PHARMACWPOtlA.
ReouirM 4 per cent of ethyl nitrit*.
I 2, eomp^ to pronounce M Munpk. oont*imng Urn than I 7» P" ^
of ethyl nitrite V7d«lt«»ted under •ection 7 of the Adulteration Act (R.8. 1906.
oh*p MaS)^ known that ihU preparation grwlually lo«s. '»■ •»'»"«»»» ^.^^^S J^
fact 1. exiXly .UUd In the fhaVmacop«ia.. It follow, that druggist, ^Id Uke
Dm«r nKtlon-to enable then, to guarantee the article which they di.pen«.. m
S^nBTu^lThT minimum .trength offloially r«,uired. It will be .een that four
m Si "«'i'Sl " oUin no eihyl nitrite whitev.r ; while (16) fifteen other. eonlUUn
•..StalfTone per cent. A phyician pr^ribin« .uch an article woul.l M.ur«l y
bTdSTppdnted In r^lU ; and whin we bear in mincT that th.. drug u. ' much u*ed in
tabriU SttoD.,to produce critical .weating; a« a diuretic to relieve strangury
pSu^by «ntb»ri«L,inall painful .««;tion. of the urinary apparatua, whether
S^toSd L3c«lou. or Inflamlnatory duordcr., and in affection, of the k.d.«»yN m
^^k~!««2*i„n of tiMMie on»n. occur. and to quiet nervou. agiUtion,' we
ct.'lZrS'r!e^rt.X"d'anl?rtothe public which* I. involved in the failure
of druggicu to keep thU drug up to pharmacop<B» sUndard..
The lamplea now reported are cbMiifled a« follow. :— 'Btmtlm.
gg
Genuine -•
Adulterated _J^
ToUl "
It thu. appear, that above 63 per cent of thew sample, are adulterated.
S,; l!l!lt SS^iination of SpiritH of Nitrou. Ether w« made iu 1891, and the re.ulU
publiHhed in Bulletlu No. 23. On that ocoasion nine (9) Mmple. wore examined, and
of thw article »iuc6 it i. ao liable to lose strength on keeping ; enpecially when the
«ni^n« ia frequently opened. The late Mr. H.rriaon reporting «I«n «»?»-
^nSned by h^ in 1891, «ya:-'8ampleH which I prepared according «« '»» B^ J;
proc^isan/keptin glaM-.toppered bottle.. enUrely filled, "^^ «"''" ^.l A wll
ker^ione yiar; but after the bottle wa. opened, and on u.mg out of I <i«ly. >»
gX^Wde^^rio^ted, ^ that I think it ought .to be kept m ^'}^^^'^^^'i'Xt^t
S!d with gl.M .topperi and of such rize that it will be d>.po«xl of in about a fortnight
after being opene<f.' i b.ve th. honour to be. Sir,
Your obedient servant,
A. McGILL,
Chief Analyit.
BULLETIN Vo. 167— MPIRITU8
VtMnr* n( Miunpi*.
Nmih'
i Athlnaa
VtMior.
CiMff,
1
I
Nmb* mmI AdrfmM ul
Mumfntiiim nr Kiirtiwhrr
M fi*Mi Ity VMHiur.
DisnticT or HOVA noon*-
IMt.
Ool ISSuiritodiitnnuiiitbKr
» »
.. U
.. 16
M 16
*I7M 0«.. Friend, Hjrdwy, N.8.1» «
33r!aJ.J.TiirnlHiil.SyrJnw,N.H. » ..
W758Cn>w» Bn»., Tniro, N.M. . 3 ,.
S37M K. A. Smith, Truro, N.H. 8 ..
I6RI6A. V. ltemt.WolfrtU«,N.8.3 ..
l»N*t Dru«. Cn.,Halltex,I(.M.
Z) R. Mfri'k, (lamisny
an I'nknown
86; K, lilvfok
t
DI8TRICT or PRINCK RDWARU MLANIV-
ObL WSpirUofnitrouiirthn
31411 N. R. Rovyrr, Cnt|«iKi. . . .
31412 J. ft G. .UnicMm, Chw
U>tt<>k>Hrn
31413.1. E UklUni, Tiini>h. ...
31414 MoKayrtcii ft NIcUIIm,
Huiiiiii«niifl«.
31415 Edgu Krir, Kmningtun, . .
So*
3
I
30 hjnuM Bniwft 'Jo., Moalrwl
aa; » H ..
3n'N»t. l>rtw Co., HiUilM, N.H.
30 Cm. Dtng Ca, St. .loha,
I N.a
SO; Howard ft Boa, HirUlord,
Kof.
DISTRICT or NKW BRUNSWICK-
Oct.
1»<
•(
31
Nov.
6
..
7
••
18
Hpirit of nitroni ether
1W44 N»t Drair »nd ChMnic«)|3 o«
1 Co., ftt. 'Itihu, S.B.
2»846iWm. Hawker ft Son, St.
.Inhn. N.B.
29fl46 (ieo. (). Hnenoer, Monct'in,
I N.U.
3SIM7|T. J. Ihirick, Newcwtir,
i X R.
a»84ttiChM. A. Burohill, Frad 3
ericwD, N.B. |
26 Nat. UniiraiMi Chemical Co.,
St John. N.&
M Howard ft Hunn, StrMfoni,
Eng.
30 Not known
% Kvaoa 8cai ft Ca, Londui,
KtlB.
30, N a. 1 initr and Chemical Ca ,
I iW. Joan, N.B.
DI><' iICT Of
BBEC-
I
Oct 31 Hpirit (rfnitruiK ether 3447)*
.. 21
.. 81
Nov. 9
S
3447M
344HI
3M91
34492
F. E. Gilbert Kiviere do 8 ni.
I^IUJI.
S. O. Clouthivr, Kivient dHjS ••
Loti|<. I
Win. Kane, Riviera du 8 „ .
Lmip.
Arthur Gagmin, Mnmy 4 ..
Bav, I
Dr. T. A. Lapuinte, Mnrray :fl « .
Bay.
WiLyMtto ft Hot
lontreal. . .
' ie, t^ielxic
Lynum & !* =iitr»a!
SS'W. r.rm..t
46
3&
DISTRICT OF ST. HTA= ^t«S-
Oet 8 Spirit of nitroas ether;
„ 13;
„ 141
., 16, ,. ...
., so<:
Rm .1. S. Trnmble, M<mtn«l. |3 ox
HKlOmer St Amour, Ste. 3 .,
I Agathe den MontH.
ItHgT. GaHd.-t .Jolirtte I? ..
»Sap. IXimiilt, 73 St C»th<.r-;3 .,
I ine, Vianville. |
884iH. W. Reynulda, MontreiU.S ..
36 Lynun Soiiii ft f,
28i
36i Lyman Knox A
I Rial.
K'Not known,
^r«!a1
ARBBRIS NITROtl.
Ina|»elor't Rctiorl
mmmn or A»u.nm.
ill
•ad Opiafaa ol tl
CbMAaiUjrrt.
R. J. WAUOH. INBPKrroR.
41
170
BM
TU
p,o.
4
I
I
B
7
IKS.
t'7B|lT|itomiainamitaadM<l.. .lOMuiw.
I'MBdvw ■iaioram MMMiard.. . .{AduttwatMl.
t MJUp to aJaiBHUB liaadMd. . . . i.>«aiiia«.
THO& MOORI, 1N8PI0T0R.
J. a FBROUSON, IN8PKJT0R.
LabriMbjroomiMuiy..
4
seo
BW
FuraulMd ti> vmdor by Nkt W
Drag knd Chemioal Co.
SMopk ftU«d from <mfiiutl| B 48
pMkm*.
4»
SB
8-8
8S
BB
l-TS'UptoitaadMtL.
198
Sll
S»
too
Baiow miaimum utaadaid..
Dp to itoDdaid.
0«aoia*.
Adaitent#d.
Genuine.
K. BELAND, IN8PKCTOR.
300
SOO
00
SOO
0-78
100
00
0-7S
00
Below miaimun Handnrd.. .
Adulterated.
J. O. BOULBAU. IN9PB0TOR.
IW
43
308
300
1»
04
3-1
30
90 0-3 o'or
0-ao
OIB
077
0-78
Bdow BUEimnm'etaBdud..
Adulterated.
•'I
M70— 2
BULLBTIN No. 167-HPIR1TU8
N»tui« i4 HmbH'-
3
i
NmiK'
Wmtor.
ManurMiuntr or FurnbhOT
M pn rn lijr Vvadur.
IIIHTKIOT or MONTRKAL-
I
0«t. 6H|iifitu(Biti»HMeHi»r 3277n Wright * C„ St. Jo»ii»,8<w
88777 r. Krc»M">'»lw. S<>r«l, ytio. a "
' HTTtt'ljir. . «nwli»ll», Bur*!, I '
1 «' I
ai77»F «hwbruoke..,S >
a
„
•
H
» 9
-•
9
.WHO' 1 1.
B, Sherliruoka..'S
Sri<, 30,»|.iri»i>liiitrm»eth«: WTOl Dr.-I. W. Mtlntwh. V«nk. 8 o«.
I In'k Hill.
. . ! S37P'.' .lolin Cliaimonhoiiar, Egnn 3 "
ville.
mua l>. J. Hiti», Krnfrew 8
V> l.yniMi (*■>!>■ * ('•>., MnnliMl
3(1 Nut kni>wii
iftLjrniMi, Knu« ft Co., MonI
rral.
Sb N»t. Itnkg Slid ni<«ii»t Co..
Ltil., M< ntrml.
8) Noi known
I
lH><rKIC!T OF OTTAWA—
ti Lynun H<«> ft Co., MontiMl
2& Nat. Dmii Co., Ottawa
2S'Not known.
Vi
13
33704 W. A. Hwidervm, Ottawa. S
SSnxvThui. A. Bruwnlt^, Ottawa 3
Oct. 3»Sp'
,. 211
Nov. 3
3
4
^fnitnmlll•th•lr .'itilCH K. Iloajt, KiiiKnton 3 oi.
. . :t»lir;7 A. V. Ctiown, KiiiK«ton... , 3 .■ .
. .tcnrSO. Wiitwm, I'nrt Hope 3 ., .
»iWtl H. \V. Mitihill.Awt HoiieS .1 .
„ .. :ilMM>iC <irt«i>ry, Lindmy 3...
Oct. 23;Spttit(ifnitrou»ether
to Ottawa l>nif Co.. Ottawa . .
9i| Nat. Drufand ChrmicalCo.,
i Ottawa-
DISTRICT OP KINU8TON-
2»i
2ti:
3!
38H6'HennCT«v l>ni(t Store, Ltd., 3 at.
Hauiilli'ii. I
3<iU7 Hurry 1". l*tt.r. Hamilton 3 .. ,
36148 H. A. Kowluiiil, Toronto. i8 ..
:«il4',t K. U. Horillnn, T.ironti 3 ..
3l>tS<>S. H. Pretty, Timmto 3 ..
I
Oct. TiSpirit of nitroun ether SOWOCeii. M. McKemlr^k, Kin- 3 ux.
cnrdiiiH.
3061O L. A. Hnckinic, Liat'ivell. .3 .. .
13
30B2I) W. A. MiConnell. Clinton 8
. 80'.IH4:H. a. HickK, (}<xl..rich 3
.1 .•»W!l.t.r. M. Httniilton, BIythe... 3
. 309».'> Walter McKibbon, Wing-;3
i ham. I
.1 30614 Chas. Aljerhart, .Seaforth . . 8
H. Skinner, Kinpton .
Nat. I)ru(t Co
Lynmn, Toronto.
DHTBICT or TORONTO-
. SOboni. UrugCo., Ltd., Haniil-
I I too-
.1 2R!
IS Lyman liron. & Co., Toronto
VadingC
15 Nat. I)riiK<V,ToronU.
l^ymi
30 The I)niK Trading Co.,
15 Nat. I)riiK<V,Toront
DISTRICT or LONIHJN -
SOU. Winer ft Co., Hamilton .
1ft Vendor
16:Canada Drug Co., London. .
SONot known
30 Nat. Drug Co.. London, Ont.
30The Drug Trading Co., To-;
i ronto.
SOiLyman Broa. ft Co., Toronto
ABTHBRIM NITR08I.
Hmmm or A.nAinm,
liM | »» et uT'» H <j>H
lUiaMka,
mit Opiaim ul (N«
J. J. oocrrioAti, inspcctur.
17«
1 46<
to;
i iH
1 I
; 1 M|
JrArRioKBYTllWPECnJR.
IT
16
*
t •
11
0-<lt Baiow oaniBiiuB lUUMburd.. . . A<ittllM*M4.
0'86l ..
0'» .. 1
l'79'U|i to minimnni (tawdard. . . acnuinr.
W.IWIow luiDimuni ■Unditrd.. . . | AtiultwiOod.
Hold M H'i'i'' "f nittom Mbar
»i«^
Htock IwuRht from Utmmt
uwiirr ; miUI »• imtv nitruiu:
rther. i
Vriiflor tmyi) uxic. «iit, aithJ 9 S4
nit. mmI ililiitH with
•tnmgrr iilciihi>l ; nold Mi
>l>t Hitli. nit. I
thUu tut nitt. ifth. nit
OT
OS
9 3
•'3
J6
Oil
saft
S'St
OS U07
B»l»w minimum nUmlkitl.. . . AJult«r»t«i
n II ' ' ' '
Up to MwdanL jGwtniM.
Balow minimum utandnrd.. . . ; Adttlt<;n>t«l.
JAK HO(»AN, INSPECTOR.
10 00^
:; fill
CO
74
100
3 6
06
07
Tnnw. Tnwe. Tr»w.
8'8I I7p to itandard Grauiao.
1 SI Below minimum ptanditrd.. . . ; Adultwatwi.
CM .. ....
20 » ....
H. J. DAtJKR, IN8PKCTOR.
|l.C ! i>.o.
4 sol 4 18
loi 1 1
i 461 2 6
6 411 6-4
Tmx'. Truce.
i
P-e. j
04 Below
•■9ll ..
IWiUpto
Tmc*. Below
Genuinv.
AdultmtMl.
Genuine.
Adulterated.
T. HkDD, INHPEOTOR.
Sample ptirohued from a boy
who aaid they made aame
themwivee.
1 96
00
1 70
4
5 60
6 60
3 80
18
00
17
04
36
,150
0-66 Below minimum (tandard . . . 1 Adultented.
00
0<2
016
1 28
2 fM
3-8 ! 1-38
Up to
Below
.Genuine.
I
....j Adulterated.
W'
BULLETIN No. 167— SPIBITUS
.
Nature of Sample.
!
"S
i
Name
and Addren of
Vendor.
Co«T.
1
i
1
Name and Addren of
Manufacturer or Fumuber
a« given by Vendor.
DISTRICT OF WINDSOR—
Oot
Spirit of nitroun ether
34«81 F. H. Laing, Windtor
34052 W. A. Fond, Windsor
346M U. O. Fleming, Windsor..
34K67 Jno. P. Jepaun, Windsor. .
34658,L. O. EgKelton, London,
East.
3 oz.
3 .. .
3 M .
3 .. .
3 .. .
Albany Chem. Co
Nat. Drug Co., London. ....
Dom. Drug Co., Hamilton..
J. P. Jepeon
Not known
DISTRICT OF MANITOBA—
Oot. 28
Spirit of nitrons ether
28
35702
35703
Vrooman k McCullough,
Winnipeg.
Speer-Stevenson Drug Co.,
Winnipeg.
3 oz.
3 .. .
35704 E. Nesbitt, Winnipeg 3
36705 Austin's Drug Store, 3
I Winnipeg.
35706 Percy K. Braund, Winnipeg
Not given.
25 E. Nesbitt, Winnipeg, Man.
25!W. R. Austin, Winnipeg,
Man.
25:The Ball Drug Co., Winni-
peg, Man.
DISTRICT OF CALGARY-
Nov. 26 Spirit of nitrous ether 3.>i7ri
35477
SO
35478
85479
35480
B. F. South, Medicine Hat 3 oz.
Higinbutham & Co., Leth- 3 h
bridge.
.F. J. Johnston, Lethbridge 3 .. .
Allierta Drag ft Book Co., 3 .. .
Lethbridge. I
C. A. WaUace, Calgary.. . . |3 .. .
30
Mbnny Chem. Co., Albany.
Lyman Sons ft Co., Montreal.
J. Winer ft Co., Hamilton. .
DISTRICT OF VANCOUVER-
Oot.
Spirit of nitrous ether
34353,McDuffw Bros, ft Co., Van-
! uouver.
3435»Only Drag Store, Van-
' couver.
343UCentral Drug Store, Van-
! couver.
34356 Haugh tons Drug Store,
1 Vancouver.
34357;R. H. Morrison ft Co.,
I Vancouver.
3 oz.
3 .. .
Not known .
Evans Sons, Lescher ft Webb,
Montreal. *
Evans Sons, Lescher ft Webb,
Liverpool, Eng.
Henderson Bros., Vancouver
25 Nat Drug Co., Vancouver. .
DISTRICT OF VICTORIA-
Nov. 30
30
,. 30
.. 30
» 30
Spirit of nitrooi ether
3»2S2|Wm. Jackson ft Co., Vic-
toria, B.C.
W. S. Terry, Victoria, B.C.
39253
39254
39250
38256
D. E. Campbell
F. J. Williams
Gea A. Eraser
3 oz.
3 .. .
3 .. .
S ..
3 ..
35Baia8 Bros, ft Stevennn,
Ltd., London, EC.
25 MalUnckrodt Chem. Works,
St Louis, U.S.A.
25 Howard ft Sons, Lond., E.C.
40 Vendor
25 Evans Sons, Lescherft Webb,
I Liverpool, Eng.
:iiL-
iETHERIS NITR08I.
R18VI.T8 or Analtms.
InspHCtur's Keinrt.
1*5
Ramuki,
M>d Opinion of the
Chief Analyst
.INO. TALBOT, INSPECTOR.
Made from ooncentnted ether
704
70
2S5
6 10
« 1
222
2 1«
22
080
8 10
9 1
3'31
S90
3-9
1-42
Up toBtandard
Below minimum atandard . .
Genuine.
Adulterated
Genuine.
Up to atandard
Bekiw minimum atandard . . ■ Adulterated.
A. C. LARIVIKRE, INSPECTOR.
Sample from a bottle labelled
Bweet«pirit« of nitre. Speer-
Stevenoon Uruft Ca , Winni
pen, Man.
3 80
40
6 80
6 00
3 54
3-8
»'4
5-8
60
35
1-38
342
2 11
2 18
Below minimum standard .
Up to Atandard
Below minimum atandard . .
Adulterated.
Genuine.
Adulterated.
R. W. FLETCHER, INSPECTOR.
7 80
1 W
920
2 Oil
1 80
78
18
92
20
18
2'84 Up to standard
O'StJ Below minimum standard.
3-35Upto itandard
0'73 Below minimum atandard.
0-66
Genuine.
Adulterated.
Genuine.
Adulterated.
.1. F. POWER, INSPECTOR.
1 44
1-4
0'6l Below minimum standard. . .
Adulterated.
564
5-5
a 00 Up to sUndard
Genuine.
360
»-5
1 ' 28 Below minimum standard . .
i
Adulterated.
290
2-9
iJ
"
686
5-9
2 16 Up to standard
Genuine.
D. O'SULLIVAN, INSPECTOR.
3 40
3-4
1 24
566
5-6
204
260
10 24
6 12
26
102
6 1
095
871
1 86
Below minimum standard. . l.'Vdulterated.
Up to standard Genuine.
Adulterated,
Genuine,
Below minimum standard .
Up to standard
minimum standard .